Semiconductor Detector Development and Processing Lab (SDDPL)


Instrumentation division’s Semiconductors Detector Development and Processing Lab (SDDPL) has been the main R&D center for development and production of prototype radiation and particle detectors (RPD) for various nuclear and high energy physics experiments at BNL and other sites (e.g. CERN) around the world. Its state of art design and processing facility for RPD is the only one in the United State with industrial and universities/other national labs included, and is one of the few in the world. We are capable of the entire detector production, which includes simulation of processing and device electrical behavior, detector and mask design, all the necessary detector processing steps (from oxidation to photolithography to metallization) except ion implantation (which we get from an outside service with a turn around time of 3-5 days), and detector testing and characterization.


SDDPL rotating caption


Personnel

  • 2 physicists with background and experience in semiconductor device physics and processing.
  • 1.5 engineers for detector processing
  • 1 technician for facility maintenance and support
  • 2-5 physicists/visitors from other department/institutes/universities working on various on going projects.


Facility and Tools

2-d Simulation tools:

Processing simulation tool allows one to go through the entire detector processing even before a single wafer is handled. This step would help one to understand the physics of detector processing and identify and eliminate potential problem before the actual processing. Key features of the simulation tool include doping profiles of various ion implants. Device simulation tool allows one to check the detector behavior under the working biases even before the processing and the testing. This step would help one to understand the detector physics under working condition and prevent potential failures of detectors before it is to be processed. Key features of the simulation tool include profiles of electric potential, electric field, and carrier concentrations. Fig. 1 shows a 3-d plot of the electric potential distribution, with electron concentration contour, in a silicon drift detector for STAR at RHIC.

field plot.jpg (39633 bytes)

Fig.1 3-D electric potential distribution electron concentration contour in a STAR drift detector.


Detector and mask design:

AutoCAD design software with multi-layer capability. Mask set for detector processing is obtained from an outside vendor using SDDPL design.


Cleanroom and processing equipment :

The new Class-100 cleanroom, shown in Fig. 2, has been in use since June 1996. The 600 sq. ft. room includes fully-instrumented wet benches, hot de-ionized water, better ventilated photoresist spinner, larger gowning area with pass-through, megasonic cleaning, automatic photoresist coating track, double-side photolithography mask aligner, two-target sputtering system with back-sputtering capability installed which allows double metal processing, exterior furnace installation, and a large capacity nitrogen boil-off system. Conditions inside the room, with constant temperature and humidity, are monitored by a central control unit. Verification of Class-100, or better, operation has been achieved. Supporting systems include laser wafer cutter and automated wire bonder. We currently have 4" wafer processing capacility, and is now ready for 6" wafer capability by June 2006.

cleanroom.jpg

Figure 2. New Class-100 cleanroom for state-of-art detector processing.

Test facilities:

After fabrication, detectors can be tested using our testing and analytical facilities:

  • Standard probe station for I-V, C-V tests on test diodes
  • Probe-card testing facility for STAR drift detectors (Fig. 3)
    Image3.gif

    Fig.3. Probe-card testing station for STAR drift detectors

  • Standard probe station for I-V, C-V tests on test diodes.
  • Defect analysis systems (Fig.4a and Fig.4b): I-DLTS, TSC, and TCT, with laser lights for carrier Generation (mainly used for identification and analysis of processing-related defects and irradiation-induced defects.
  • TSC.jpg

    Fig.4a. I-DLTS/TSC system

    TCT.jpg

    Fig.4b. TCT system

DETECTORS MADE AND CURRENT PROJECTS


Various types of silicon detectors, including micro-strip detectors, pad detectors, drift detectors, and pixel detectors have been made over last 10 years for application in high and nuclear physics experiments and X-ray detection. Table I is a list of many of them with application and status:
Table I Detector Fabrication Status SDDPL
Detector Application Results/Status
400 element pad detector, ceramic overlay; three sets of charge-divided strips NA 34 (CERN) Used in exp. For three years Beuttenmuller et al. NIM A252 (1986) 471
512 element pad detectors, large and small interior holes E814 (AGS, BNL) Used for several years as multiplicity counter Giubelino, et al., NIM
192 element pad detectors square array TRD test Used at CERN for several years (V. Polychronakos)
192 element pad detectors square array NA44 (CERN) Used at CERN for several years (V. Polychronakos)
3 in diameter cylindrical silicon drift detectors NA 45 (CERN) First drift detector application Chen et al., IEEE TNS NS39, 619(1992), NIM A326 (1993)
STAR 6.3x6.3 cm 2 silicon drift detectors ( Fig. 5 ) SVT for STAR at RHIC Prototype detectors for 216 detector SVT array finished Now in production at BNL and SINTEF (on-going)
50 micron pitch strip detectors Muon Beam Finder (CERN) In use for two years in M2 test beam (V. Polychronakos)
2 and 8 micron pitch strip detectors Accel. Test Facility, BNL Production used PdSi method Z. Li et al., IEEE TNS NS38 (1991)
50 micron pitch strip detectors Current AGS To be installed L. Remsberg, V. Polychronakos
PHOBOS test detectors PHOBOS at RHIC Polyimide coating test, FOXFET structures Ryan, Busza, MIT
120 element array high-rate EXAFS detectors NSLS X19 Successful tests with 16 elements Pullia et al., NIM, BNL-62142, 62735 (on-going)
16 element strip for diffraction NSLS Siddons, to be installed
Radiation effects test diode gamma ray irradiation BNL gamma source Kraner et al., Italian Phys. Soc., Vol. 46, Baldini ed., Bologna (1994)
Radiation effects test diode Displacement damage effects Fast neutrons Z. Li et al., numerous publications,Still on-going
p- type pixel detectors (n+/p/p+) 48µm x 192µm pixels 120x8 array 96µm x 96µm pixels 16x60 array Prototype for CMS at LHC Lander, UC Davis Under test, on-going Z. Li et al., BNL-64488, to appear in NIM
n- type pixel detectors (n+/n/p+) 125µm x 125µm pixels 24x32 array 250µm x 62.5µm pixels 12x64 array ( Fig. 6 ) Prototypes for CMS at LHC Chien, Johns Hopkins Univ. Under test, on-going Z. Li et al., BNL-64488, to appear in NIM W. Chen et al., BNL-64979
fig6.jpg

Fig.6 n- type pixel detector

n- type pixel detectors (p+/n/n+) 20µm x200µm pixels 24x32 array ( Fig. 7 ) Fermilab D0 Anderson, Kwan, Fermilab Under test, on-going Z. Li et al., BNL-64488, to appear in NIM W. Chen et al., BNL-64979
fig7.jpg

Fig.7 n- type pixel detector for D0 at Fermilab

100µm pitch large-area strip detectors 37 cm 2 sensitive area AC coupled with implanted biasing resistors ( Fig. 8 and 9 ) Prototype for PP2PP at RHIC Guryn, Physics To be tested at Fermilab On-going
fig8.jpg

Fig.8 100 µm strip detector

fig9.jpg

Fig.9 100 µm strip detector

Drift detector array for high-rate EXAFS NSLS X19 Siddons, NSLS, to be tested On-going
X-ray active matrix pixel sensor (XAMPS) for X-ray crystallography and STEM recording data NSLS & Biology Department ongoing W. Chen, Z. Li, P. Rehak, J. Wall (Biology) and P. Siddons (NSLS)
P- type drift detectors for Lunar mission NASA Lunar Mission (MSFC) ongoing/Brian Ramsey (NASA), W. Chen, Z. Li and P. Rehak
Novel Si Strippixel detectors for PHENIX upgrade (SVX) at RHIC PHENIX at RHIC, RBRC, RIKEN Z. Li, H. En'Yo et al. NIM A518 (2004) 300-304
Novel Si Strippixel detectors for PHENIX upgrade (Calorimeter) at RHIC PHENIX at RHIC, RBRC Z. Li, E. Kistenev, et al.

RADIATION DAMAGE EFFECT HARDNESS STUDIES



Silicon radiation detectors continue to be applied to nuclear and high-energy physics experiments in both increasing complexity and quantity. Detector radiation hardness against displacement damage has become a major issue in the development of silicon tracking detectors for high-energy physics experiments in the LHC.


We have been studying the effects of fast neutron and ionizing particle radiation on the electrical properties of silicon radiation detectors, which are in widespread use as position sensitive detectors in high energy physics experiments. These damage effects will be especially important in high luminosity experiments such as at the LHC. Deep Level Transient Spectroscopy (DLTS), current shape, Thermally Stimulated Current (TSC) measurements, and Transient Current Technique (TCT) reveal specific defect structures in the silicon lattice that cause increased thermally generated current (dark current), space charge transformations (or "inversion") and short and long term annealing effects. Interactions of defects with benign, endogenous impurities in the silicon material used in these detectors offer possible amelioration of the effects of bulk displacement defects and we are pursuing methods of enhancement of these impurities (e.g., Sn, C, N, O).


The defect analysis system (DLTS, TSC, and TCT), including optical defect filling techniques, has been completed and is in routine use. The "reverse anneal" effect was correlated with a deep acceptor at Ec-0.4 eV, which is usually attributed to the di-vacancy. High carbon content material was found to exhibit not very different anneal and radiation effect properties from normal material. Positron annihilation studies have been applied to neutron-irradiated silicon for the first time and an indication of clusters (voids), which break up during anneal and supply vacancies, has been observed. Measurements on Sb doped Si detectors (material provided by NREL) and high energy Li implanted Si detectors have shown improved rad-hardness of about a factor 1.5 to 2 from standard materials. We are the first group to use low resistivity silicon materials for particle detectors with improved radiation hardness, which is a leading candidate of the actual material for detector fabrication in LHC applications. We have also first developed the technology to introduce high concentrations (1017cm-3) of oxygen into FZSi. Oxygenated Si detectors, which are 2-4 times more radiation hard to charge particle (p,π) radiation. We have also developed cryogenic Si detectors (in collaboration with CERN RD39); MCZ Si detectors, in collaboration with Helsinki Institute of Physics and Loffe Institute, with much improved radiation hardness. Recently (June 2005), we have developed a new technology card DRIVE (detectory Recovery/Improvement Via Elavated temperature annealing), which can improve leakage current, full depletion voltage and charge collection efficiency for heavily irradiated MCZ Si detectors.


Continued measurements of material-engineered samples will be made to establish electronic effects of specific structures (di-vacancy, etc.). Further studies will continue in defect engineering, using samples such as Sn-doped FZ silicon wafers to fabricate radiation hardened detectors. We are a major contributor in a new R&D collaboration (RD48, the ROSE collaboration) devoted specifically to the development of radiation-hard silicon detectors for both ATLAS and CMS at the LHC.


For information about the Semiconductor Laboratory, please contact: Dr. Z. Li (631) 344-7604


Last Modified: Wednesday, 06-Feb-2013 22:33:56 EST